Loading...

Messages

Proposals

Stuck in your homework and missing deadline? Get urgent help in $10/Page with 24 hours deadline

Get Urgent Writing Help In Your Essays, Assignments, Homeworks, Dissertation, Thesis Or Coursework & Achieve A+ Grades.

Privacy Guaranteed - 100% Plagiarism Free Writing - Free Turnitin Report - Professional And Experienced Writers - 24/7 Online Support

Base extraction of benzoic acid from acetanilide recrystallization of products

01/10/2021 Client: muhammad11 Deadline: 2 Day

For the portion of the procedure shown below, create a flow chart for the acid-base extraction at the end of the Grignard Reaction. Start your flow chart with the crude reaction (see below) mixture before addition of HCl and continue it until the product is recovered. Depict the desired organic product, in its correct form at each step of the procedure.

Crude reaction mixture procedure for reference: To the flask add Mg turnings (120 mg, 4.94 mmol) to the flask followed by anhydrous tetrahydrofuran (~10 mL). Add 1-bromo-4-fluorobenzene (500 L, 4.55 mmol, dispensed via an Eppendorf pipette) directly to the flask, followed by ~5 drops of 1,2-dibromoethane. Reflux the reaction mixture for ~30 min, stirring the mixture rapidly during the process. The start of the reaction is indicated by a slight turbidity of the solution. The mixture may become more turbid as the reaction proceeds and eventually may turn a pale yellow. Allow the reaction mixture to cool to room temperature after the reflux period.

Procedure for extraction:
With stirring, add water (~10 mL) followed by aq. 6 M HCl solution (~3 mL) dropwise. Add diethyl ether (~10 mL) and stir the mixture until any remaining solids dissolve. Transfer the two-phase mixture to a separatory funnel and shake vigorously to further extract the product into the organic layer. Isolate the organic layer and extract the aqueous layer with diethyl ether (~5 mL). Combine the organic layers and extract them with aq. 5 % NaOH solution (2 × ~10 mL portions). Isolate the appropriate layer and acidify with aq. 6M HCl solution. Isolate the solid product by vacuum filtration on a small plastic filter funnel and rinse it with ice-cold water (2 × 5 mL).

Example flow Chart:

Homework is Completed By:

Writer Writer Name Amount Client Comments & Rating
Instant Homework Helper

ONLINE

Instant Homework Helper

$36

She helped me in last minute in a very reasonable price. She is a lifesaver, I got A+ grade in my homework, I will surely hire her again for my next assignments, Thumbs Up!

Order & Get This Solution Within 3 Hours in $25/Page

Custom Original Solution And Get A+ Grades

  • 100% Plagiarism Free
  • Proper APA/MLA/Harvard Referencing
  • Delivery in 3 Hours After Placing Order
  • Free Turnitin Report
  • Unlimited Revisions
  • Privacy Guaranteed

Order & Get This Solution Within 6 Hours in $20/Page

Custom Original Solution And Get A+ Grades

  • 100% Plagiarism Free
  • Proper APA/MLA/Harvard Referencing
  • Delivery in 6 Hours After Placing Order
  • Free Turnitin Report
  • Unlimited Revisions
  • Privacy Guaranteed

Order & Get This Solution Within 12 Hours in $15/Page

Custom Original Solution And Get A+ Grades

  • 100% Plagiarism Free
  • Proper APA/MLA/Harvard Referencing
  • Delivery in 12 Hours After Placing Order
  • Free Turnitin Report
  • Unlimited Revisions
  • Privacy Guaranteed

6 writers have sent their proposals to do this homework:

Coursework Assignment Help
Innovative Writer
Ideas & Innovations
Top Class Results
Solution Provider
Coursework Help Online
Writer Writer Name Offer Chat
Coursework Assignment Help

ONLINE

Coursework Assignment Help

I will cover all the points which you have mentioned in your project details.

$35 Chat With Writer
Innovative Writer

ONLINE

Innovative Writer

Give me a chance, i will do this with my best efforts

$26 Chat With Writer
Ideas & Innovations

ONLINE

Ideas & Innovations

I have read your project details. I can do this within your deadline.

$38 Chat With Writer
Top Class Results

ONLINE

Top Class Results

I am known as Unrivaled Quality, Written to Standard, providing Plagiarism-free woork, and Always on Time

$34 Chat With Writer
Solution Provider

ONLINE

Solution Provider

You can award me any time as I am ready to start your project curiously. Waiting for your positive response. Thank you!

$22 Chat With Writer
Coursework Help Online

ONLINE

Coursework Help Online

You can award me any time as I am ready to start your project curiously. Waiting for your positive response. Thank you!

$44 Chat With Writer

Let our expert academic writers to help you in achieving a+ grades in your homework, assignment, quiz or exam.

Similar Homework Questions

Fearless planet grand canyon worksheet - Bacon's auto salvage west memphis - TIMEMAPPER ENTRY 2 (ENCYCLOPEDIA STYLE) CAREFULLY READ ATTACHED DOC. - Personality reflection worksheet - Resistance in a wire simulation answers - Psychology unit 3 and 4 notes - Algebraic notation year 7 - Clc development powerpoint presentation - Natalie porter rapid rose tutorial - Info tech Global economy- Project Work-Implementing information technology across the globe- Week 9 - Interlink express tracking number - The Status of Global HIV Efforts - Thin lens equation problems - What are narrative conventions - What is an audience profile sheet - Research methods in psychology 2nd edition by beth morling - Biology of osmosis jones answers - How to check baggage fare in amadeus - What language technique is used in this quote - C program for round robin scheduling with gantt chart - Business requirements document template example - The moon be still as bright - Services marketing lovelock wirtz - Discussion board - Chlorsig eye ointment side effects - Abstract algebra help - How to cite a 10k report apa - Paul hartley vocational assessor - American standard code for information interchange table - Venom and spiderman fanfiction - Cloud Computing - Single system design - Chevrolet 100 years of product innovation case analysis - Brightgreen d900 shx curve - Topic: Criminal Justice -Analysis of poverty and crime. - MGT/498: Strategic Management Wk 5 - Apply: Signature Assignment: Strategic Management Research Project Presentation [due Day 7] Wk 5 - Apply: Signature Assignment: Strategic Management Research Project - Manual handling risk assessment matrix - Advantages and disadvantages of honey and mumford learning styles - The Managerial Role in Crafting and Executing Strategy - Wk#4 Research paper - Provision for annual leave journal entry - Abb dcs800 fault list - Training and Development : Unit VI Journal, Unit VI Assessment, Unit VII Homework, Unit VII PowerPoint Presentation - System development life cycle case study - Boundaryless organization pros and cons - Life cycle of an apple tree book - Statewide vision resource centre - Caterpillar 3126 spec sheet - Python program for rail fence technique - Week 12 assignment - Discussion 3 - Mr spock's avocation 7 little words - Psychology Final Grad Level - A philanthropic organization sent free mailing labels - The cold equations short story - Walkerville council hard rubbish collection - Essay fashion - Cell city phone specials - Cdk digital marketing case study slideshare - Ethics policies typically cover all of the following issues except - Ellen foster chapter 3 summary - Chapter 27 summary to kill a mockingbird - Valuation of abnormal loss in consignment - Does domino's deliver heart shaped pizzas - Data mining midterm exam with solutions - War veterans home myrtle bank - North leeds medical practice - 18-22 lakeview drive lilydale - Capsim creating a new product - Biology Week 5 - Uif declarations email address - Scholar practitioner's guide to research design - Making junk model animals - Ibm z os lifecycle - Microchannel heat exchanger ppt - Essay - Northern midlands council rubbish collection - How to create a project network diagram in excel - Coffee kiosk business plan - The welcome table alice walker short story - Carlin soskice macroeconomics solutions - Executive Program Practical Connection Assignment on Information Governance - Premodern japan a historical survey pdf - 2 coments each one 150 words (CITATION AND REFERENCE) - Hero of lion king - Self Reflection - BUSINESS INTILLEGANCE COURSE - Business name register victoria - On course study skills plus 3rd edition chapter 1 - Plastic surgery sales consultant salary - G scan 2 key programming - Examples of synthetic products - The thermal decomposition of potassium chlorate - Abhi Assignment - Covid-19 Pandemic Situation-ESA And Work From Home - Analyzing pro forma statements xyz company - D3 - Into thin air comprehension questions - Engine position system performance bank 2 - Broome north primary school address