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Experiment 10: Synthesis of Aspirin Name: Data/observations: Day 1Preparation of Salicylic Acid 1.1749 mass of methyl salicylate (wintergreen oil) 0.913 g mass of salicylic acid product Day 2: Synthesis of Aspirin 0.889 mass of salicyclic acid used to synthesize aspirin 0.622 g mass of aspirin product Day 3: Qualitative Analysis Compound pure pure aspirin salicylic acid aspirin pure salicyclic methyl acid product product salicylate purple w/ dark purple night yellow dark purple yeilow seperation crystalized crystalized watery Chunky. FeCl3 Observation
Follow-up Questions: 1 Write the balanced chemical equation for the hydrolysis of methyl salicylate using molecule formulas (not Lewis structures or line drawings). 9. Write the balanced chemical equation for the acetylation of salicylic acid using molecular formulas (not Lewis structures or line drawings). Calculations: theoretical yield for salicylic acid (Day 1) percent yield for salicylic acid (Day 1) theoretical yield for synthesis of aspirin (Day 2) percent yield for synthesis of aspirin (Day 2)
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