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Dehydration of 2 butanol lab report

14/04/2021 Client: muhammad11 Deadline: 2 Day

Hi I need someone to reword my procedures for my lab experiment (All in black only, not in red/blue) I have done the first page to show you the format that needs to be followed. It doesn't have to be reworded too extremely just small changes are fine.EXPERIMENTAL PROCEDURE: *NOTE: in the experiment video, only two reactions are performed: the dehydration of 2-butanol, and the dehydrobromination of 1-bromobutane. Prepare the experimental portion of your notebook for only those two reactions, see guidelines above and on ELN for more detail. PART A A1. Dehydration of 2-Butanol Obtain an experiment kit from the stockroom. In a reaction tube, place 2 drops of concentrated sulfuric acid. Add a boiling stone and connect the reaction tube to the gas collection assembly as shown in Fig. 4.1. Assemble the gas collection apparatus shown in figure 4.1 before the reactants are mixed. To position the gas collection tube, carry out the following steps: 1. Fit the collection tube with a septum stopper in one end. 2. Fill the collection tube with water. ​What is the purpose of the water? 3. Insert the end of the Teflon tubing that is coming out from the top of the septa into the collection tube all the way up to reach the stopper. 4. Place your index finger over the open end of the tube and invert it (water should have remained in the tube). 5. Place the tube, with the open end down, into a 250-mL beaker approximately half full with water. 6. Remove your finger (the column of water should remain in the tube.) 7. Connect the other end of the Teflon tubing to the reaction tube as shown in figure 4.1. After the assembly is complete, use a syringe to add 0.2 mL of 2-butanol to the reaction tube and heat the mixture in a preheated heating block. Do​n't assume things aren't hot. Hover your hand near the object in question to feel for heat radiating from it just like you would a pan on the stove if you weren't sure whether it was hot or not​. Generation of gaseous product can be observed by watching the rapid decrease of the water level in the collection tube. ​Keep heating until no more bubbles escape from the bottom of the collection tube. Remove the Teflon tubing from the gas collection tube, and then from the beaker, before removing the reaction tube from the heat, ​all the while ensuring your collection tube stays below the beaker’s water level. ​Why is it important that the collection tube stays below the water level? Use this sequence of steps in shutting down the reaction to prevent water from being sucked back into the hot reaction tube while it is cooling down. Label the beaker containing the collection tube kept in the water and submit it to your TA for the gas chromatographic analysis. ​Cool heating blocks between reactions.

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