Loading...

Messages

Proposals

Stuck in your homework and missing deadline? Get urgent help in $10/Page with 24 hours deadline

Get Urgent Writing Help In Your Essays, Assignments, Homeworks, Dissertation, Thesis Or Coursework & Achieve A+ Grades.

Privacy Guaranteed - 100% Plagiarism Free Writing - Free Turnitin Report - Professional And Experienced Writers - 24/7 Online Support

Introduction of recrystallization of naphthalene

26/04/2021 Client: muhammad11 Deadline: 2 Day

EXP 3-1 RECRYSTALLIZATION (MICROSCALE) UNLV CHEM 241L SUMMER 2020 RECRYSTALLIZATION: Introduction • Read INTRODUCTION and THEORY OF CRYSTALLIZATION sections in the provided lab manual. • Understand the basic concept of recrystallization • Review the polarity concept from the previous lab (solubility and solution) if necessary RECRYSTALLIZATION : Introduction • Recrystallization → a purification technique for solid compounds → the solubility of a compound in a specific solvent is the most important property • Good recrystallization solvent? → sparingly soluble at room temperature → highly soluble at elevated temperature (boiling temperature) RECRYSTALLIZATION : Experimental • Purification of impure naphthalene by two recrystallization solvents → ethanol → hexane • Determine which solvent is a good recrystallization solvent for naphthalene → based on experimental melting point provided in the video → based on the % recovery of naphthalene from each recrystallization Experiment # 3-1: Recrystallization (Micro-scale) INTRODUCTION In most organic chemistry experiments, the desired product is first isolated in an impure form. If this product is a solid, the most common method of purification is crystallization. The general technique involves dissolving the material to be crystallized in a hot solvent (or solvent mixture) and cooling the solution slowly. The dissolved material has a decreased solubility at lower temperatures and will separate from the solution as it is cooled. This phenomenon is called crystallization, if the crystal growth is relatively slow and selective, or precipitation, if the process is rapid and nonselective. Crystallization is an equilibrium process and produces very pure material. A small seed crystal is formed initially, and it then grows layer by layer in a reversible manner. In a sense, the crystal “selects” the correct molecules from the solution. In precipitation, the crystal lattice is formed so rapidly that impurities are trapped within the lattice. Therefore, any attempt at purification with too rapid a process should be avoided. Because the impurities are usually present in much smaller amounts than the compound being crystallized, most of the impurities will remain in the solvent even when it is cooled. The purified substance can then be separated from the solvent and from the impurities by filtration. THOERY OF CRYSTALLIZATION The first problem in performing a crystallization is selecting a solvent in which the material to be crystallized shows the desired solubility behavior. In an ideal case, the material should be sparingly soluble at room temperature and yet quite soluble at the boiling point of the solvent selected. The solubility curve should be steep, as can be seen in line A of Figure 1. A Figure 1. Graph of solubility vs. temperature. 1 curve with a low slope (line B) would not cause significant crystallization when the temperature of the solution was lowered. A solvent in which the material is very soluble at all temperatures (line C) also not be suitable crystallization solvent. The basic problem in performing a crystallization is to select a solvent (or mixed solvent) that provides a steep solubility-vs.-temperature curve for the material to be crystallized. A solvent that allows the behavior shown in line A is an ideal crystallization solvent. A successful crystallization depends on a large difference between the solubility of a material in a hot solvent and its solubility in the same solvent when it is cold. When the impurities in a substance are equally soluble in both the hot and the cold solvent, en effective purification is not easily achieved through crystallization. A material can be purified by crystallization when both the desired substance and the impurity have similar solubilities, but only when the impurity represents a small fraction of the total solid. The desired substance will crystallize on cooling, but the impurities will not. In this experiment, you will perform a micro-scale crystallization. Impure naphthalene will be recrystallized from hexane and ethanol separately, and you will determine a good recrystallization solvent for naphthalene based on melting point measurement and % recovery.

Homework is Completed By:

Writer Writer Name Amount Client Comments & Rating
Instant Homework Helper

ONLINE

Instant Homework Helper

$36

She helped me in last minute in a very reasonable price. She is a lifesaver, I got A+ grade in my homework, I will surely hire her again for my next assignments, Thumbs Up!

Order & Get This Solution Within 3 Hours in $25/Page

Custom Original Solution And Get A+ Grades

  • 100% Plagiarism Free
  • Proper APA/MLA/Harvard Referencing
  • Delivery in 3 Hours After Placing Order
  • Free Turnitin Report
  • Unlimited Revisions
  • Privacy Guaranteed

Order & Get This Solution Within 6 Hours in $20/Page

Custom Original Solution And Get A+ Grades

  • 100% Plagiarism Free
  • Proper APA/MLA/Harvard Referencing
  • Delivery in 6 Hours After Placing Order
  • Free Turnitin Report
  • Unlimited Revisions
  • Privacy Guaranteed

Order & Get This Solution Within 12 Hours in $15/Page

Custom Original Solution And Get A+ Grades

  • 100% Plagiarism Free
  • Proper APA/MLA/Harvard Referencing
  • Delivery in 12 Hours After Placing Order
  • Free Turnitin Report
  • Unlimited Revisions
  • Privacy Guaranteed

6 writers have sent their proposals to do this homework:

Calculation Guru
Custom Coursework Service
Top Class Results
A Grade Exams
Finance Homework Help
Assignment Guru
Writer Writer Name Offer Chat
Calculation Guru

ONLINE

Calculation Guru

I will cover all the points which you have mentioned in your project details.

$46 Chat With Writer
Custom Coursework Service

ONLINE

Custom Coursework Service

I have read your project details. I can do this within your deadline.

$21 Chat With Writer
Top Class Results

ONLINE

Top Class Results

I am known as Unrivaled Quality, Written to Standard, providing Plagiarism-free woork, and Always on Time

$22 Chat With Writer
A Grade Exams

ONLINE

A Grade Exams

I am known as Unrivaled Quality, Written to Standard, providing Plagiarism-free woork, and Always on Time

$47 Chat With Writer
Finance Homework Help

ONLINE

Finance Homework Help

I have read your project details. I can do this within your deadline.

$15 Chat With Writer
Assignment Guru

ONLINE

Assignment Guru

I have read and understood all your initial requirements, and I am very professional in this task.

$23 Chat With Writer

Let our expert academic writers to help you in achieving a+ grades in your homework, assignment, quiz or exam.

Similar Homework Questions

Angle of elevation and depression word problems - One strategy for managing debilitative communication apprehension is to - Why did donna butterworth quit acting - A clockwork orange symbols - Assignment: Case Study Analysis - Po box 1522 fortitude valley - Info tts net pk - The glass castle study guide pdf answers - Gale force surfing case study answers - Two years are better than four short summary - To kill a mockingbird quiz chapters 1 11 - Tin fluoride is often added to toothpaste - Bachelor of midwifery rmit - Trends & issues in executive management for health care administrators - Security as a service business model - The habitable planet ecology lab answers - Spying on miss muller - Subtraction snakes and ladders - Jasper jones chapter 9 summary - Don t tell em fortune remix - 21823 friendship view drive springdale ar - Supplementary services in service marketing examples - Discussion - Onslow company purchases a used machine - Apical surface of epithelial tissue - The t test for nursing - Mass effect 3 support raan or gerrel - The cremation of sam mcgee lyrics - Tessie hutchinson in the lottery - Health history and medical information - Power monitor 3000 user manual - Nutrition case study assignment - Do you think probation serves a purpose? Or is it just punitive—punishment on top of punishment? Why? - List and briefly define ieee services - 6 ferndale road glen iris home lottery - Nurs521promptw8 - Discovering physical geography pdf - Product liability - Long term care and Pharmacueticals - WEEK 8 DISCUSSION - Spelt risotto trader joe's discontinued - Could you complete a power point with 10-15 slides in Apa 7th edition format? Topic is specific leadership and management traits and theories necessary for managing a multidisciplinary and multicultural health care organization to promote organizational effectiveness. - Threat vulnerability assessment template - Walmart inc takes on amazon com case study solution - Field axioms of real numbers examples - Hambleton gov uk recycling - Vcaa physics data sheet - Ucl economics and statistics - Social Media - Study questions 2 - Founder of individual psychology - Explain why disorders caused by dominant alleles on - Spy pen camera jaycar - Advanced algorithm (python) - Econ Project - Ethnic literature definition - Tree trimming project - Essentials of negotiation test bank free - In a 4 page project proposal written to the leadership of your healthcare organization, propose a nursing informatics project for your organization that you advocate to improve patient outcomes or patient-care efficiency. This must be - Managerial Economics Discussion Needed in 8 hours - Reply to my peers - Crisis Intervention - The periodic table - Alliteration romeo and juliet - Nursing - Bode plot example problems - What are risk management standards - The slums of aspen sparknotes - ASSIGNMENT 5 - VHDL Assignment 3 - Nurse practitioner cover letter pdf - Write a 500 word movie review on : Gangs of New York - 2 page apa paper on communication - Nutrition science and applications 4th edition - Fabio old spice commercials - Magnesium oxide experiment lab report - Excel chapter 4 grader project 2018 - Imperial college of trades adelaide - Chemistry Exercises - Current carrying capacity of 2.5mm cable australia - The story of american freedom eric foner free pdf - Role of dic in entrepreneurship development ppt - Https www internetsociety org tutorials your digital footprint matters - Esol nexus going to work - Adairs gift card balance - Two particles with charges of nc - Veeder root tls 300 troubleshooting - Villanova master black belt certification - Av jennings home designs packages - Three overriding scm activities within and between firms include - Fiu marketing certificates - Group homework - Cytochrome P450 System - (1) Essay and (1) Case Study - Discussion 6B - Summary - Horizontal marketing system example - Cisco mds 9710 end of life - Module 7 sam project 1a - Complete Information About Tips